(-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol

Base Information

Chemical Name:(-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol
CAS No.:946419-58-5
Molecular Formula:C₃₈H₄₆O₇
Molecular Weight:614.779
Hs Code.:

Synonyms:(-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol

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Chemical Property of (-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol

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Technology Process of (-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol

There total 4 articles about (-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 15424-04-1
2-(allyloxy)ethyl bromide

: 946571-76-2
(+)-D-1,5-bis-O-allyl-2,3,6-tris-O-benzyl-myo-inositol

: 946419-58-5
(-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 0 - 25 ℃;
DOI:10.1021/jo070611a

Reference yield:

: 946419-42-7
(-)-D-1,5-bis-O-allyl-2,6-bis-O-benzyl-myo-inositol

: 946419-58-5
(-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Bu₂SnO; nBu₄NI; molecular sieves 3 Angstroem / acetonitrile / 24 h / Heating

2: 80 percent / NaH; nBu₄NI / dimethylformamide / 0 - 25 °C

With 3 A molecular sieve; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo070611a

Reference yield:

: C₃₆H₄₆O₆

: 946419-58-5
(-)-D-1,5-bis-O-allyl-4-O-[2-(allyloxy)ethyl]-2,3,6-tris-O-benzyl-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / acetyl chloride; methanol / CH₂Cl₂ / 4 h

2: 71 percent / Bu₂SnO; nBu₄NI; molecular sieves 3 Angstroem / acetonitrile / 24 h / Heating

3: 80 percent / NaH; nBu₄NI / dimethylformamide / 0 - 25 °C

With methanol; 3 A molecular sieve; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; acetyl chloride; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo070611a