C₃₆H₄₅NO₈

Base Information

• Chemical Name: C₃₆H₄₅NO₈
• CAS No.: 1276112-31-2
• Molecular Formula: C₃₆H₄₅NO₈
• Molecular Weight: 619.755
• Mol file: 1276112-31-2.mol

Synonyms:C₃₆H₄₅NO₈

Chemical Property of C₃₆H₄₅NO₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₄₅NO₈

There total 12 articles about C₃₆H₄₅NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C33H41NO6 (1276112-30-1) + chloroformic acid ethyl ester (541-41-3) → C36H45NO8 (1276112-31-2)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

C27H27NO5 (1308271-84-2) → C36H45NO8 (1276112-31-2)

Guidance literature:

Multi-step reaction with 7 steps

1: sodium tetrahydroborate / methanol / 24 h / 0 - 20 °C

2: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

3: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 2 h / 0 °C

5: tetrahydrofuran / 1.5 h / -78 °C

6: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 2 h / 0 °C

7: pyridine / 12 h / 0 - 20 °C

With pyridine; dmap; sodium tetrahydroborate; ammonium cerium (IV) nitrate; cerium(III) chloride heptahydrate; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

C27H29NO5 (1308271-86-4) → C36H45NO8 (1276112-31-2)

Guidance literature:

Multi-step reaction with 6 steps

1: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

2: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

3: dmap; triethylamine / dichloromethane / 2 h / 0 °C

4: tetrahydrofuran / 1.5 h / -78 °C

5: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 2 h / 0 °C

6: pyridine / 12 h / 0 - 20 °C

With pyridine; dmap; sodium tetrahydroborate; ammonium cerium (IV) nitrate; cerium(III) chloride heptahydrate; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1016/j.tetlet.2011.01.018

upstream raw materials:

C₂₇H₂₇NO₅

C₂₇H₂₉NO₅

C₃₄H₃₅NO₅

C₂₆H₂₇NO₄

Downstream raw materials:

C₃₃H₄₁NO₅

C₃₂H₃₉NO₆

C₃₃H₄₃NO₇

C₃₅H₄₃NO₅