benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide

Base Information

Chemical Name:benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide
CAS No.:1357168-38-7
Molecular Formula:C₂₅H₂₆N₂O₆S
Molecular Weight:482.557
Hs Code.:

Synonyms:benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide

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Technology Process of benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide

There total 8 articles about benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 25054-53-9
3,4-(methylenedioxy)benzoyl chloride

: 1021926-19-1
C₁₇H₂₂N₂O₃S

: 1357168-38-7
benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide

Guidance literature:: With potassium carbonate; In 1,4-dioxane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.11.012

Reference yield: 71.0%

: 1357168-38-7
benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide

Guidance literature:

Reference yield:

: 930797-62-9
2-(2,5-dimethylbenzyloxy)-4-nitroaniline

: 1357168-38-7
benzo[1,3]dioxole-5-carboxylic acid [3-(2,5-dimethylbenzyloxy)-4-(N-methanesulfonyl-N-methylamino)phenyl]amide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: water; sodium hydroxide

3.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: iron(III) chloride; water; zinc / N,N-dimethyl-formamide

5.1: potassium carbonate / 1,4-dioxane / 20 °C / Inert atmosphere

With iron(III) chloride; water; sodium hydride; potassium carbonate; sodium hydroxide; zinc; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.11.012