1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane

Base Information

Chemical Name:1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane
CAS No.:76980-35-3
Molecular Formula:C₃₅H₅₁N₃O₁₂S₅
Molecular Weight:866.133
Hs Code.:

Synonyms:1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane

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Chemical Property of 1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane

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Technology Process of 1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane

There total 5 articles about 1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 124-63-0
methanesulfonyl chloride

: 76980-34-2
4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane-1,15-diol

: 76980-35-3
1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/ja00395a077

Reference yield:

: 56-18-8
bis(3-aminopropyl)amine

: 76980-35-3
1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / K₂CO₃ / H₂O / 3 h / 60 °C

2: K₂CO₃ / dimethylformamide / 80 °C

3: 71 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

4: 97 percent / Et₃N / CH₂Cl₂ / 1.5 h / -18 °C

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19830660426

Reference yield:

: 35980-64-4
1,5,9-Tritosyl-1,5,9-triazanonane

: 76980-35-3
1,15-di(methanesulfonyloxy)-4,8,12-tri(p-toluenesulfonyl)-4,8,12-triazapentadecane

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 80 °C

2: 71 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

3: 97 percent / Et₃N / CH₂Cl₂ / 1.5 h / -18 °C

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19830660426