(4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal

Base Information

Chemical Name:(4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal
CAS No.:154777-14-7
Molecular Formula:C₁₈H₂₅NO₃S
Molecular Weight:335.467
Hs Code.:

Synonyms:(4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal

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Chemical Property of (4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal

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Technology Process of (4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal

There total 3 articles about (4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 36255-44-4
3-bromopropanal dimethyl acetal

: 139437-48-2
(R)-2-phenyl-(2-thienylmethyleneamino)ethanol

: 154777-14-7
(4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal

Guidance literature:: With magnesium; In tetrahydrofuran; for 15h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80819-X

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 154777-14-7
(4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / benzene / 4 h / Heating

2: 58 percent / 1.) Mg / tetrahydrofuran / 15 h / Ambient temperature

With magnesium; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)80819-X

Reference yield:

: 56613-80-0
D-2-phenylglycinol

: 154777-14-7
(4R-1'R)-4-(2'-hydroxy-1'-phenylethylamino)-4-(2-thienyl)-butanal dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / benzene / 4 h / Heating

2: 58 percent / 1.) Mg / tetrahydrofuran / 15 h / Ambient temperature

With magnesium; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)80819-X