dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate

Base Information

Chemical Name:dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate
CAS No.:1351221-60-7
Molecular Formula:C₂₂H₃₂B₂O₈
Molecular Weight:446.113
Hs Code.:

Synonyms:dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate

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Technology Process of dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate

There total 6 articles about dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 90841-95-5
dimethyl 2,5-diiodo-1,4-benzenedicarboxylate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1351221-60-7
dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; triethylamine; In toluene; for 12h; Reflux; Inert atmosphere;
DOI:10.1039/c1jm14682c

Reference yield: 38.0%

: 90841-95-5
dimethyl 2,5-diiodo-1,4-benzenedicarboxylate

: 73183-34-3
bis(pinacol)diborane

: 1351221-60-7
dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate

Guidance literature:: With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 20h; Inert atmosphere;
DOI:10.1039/c1jm14682c

Reference yield:

: 120-61-6
1,4-benzenedicarboxylic acid dimethyl ester

: 73183-34-3
bis(pinacol)diborane

: 1351221-60-7
dimethyl 2,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)terephthalate

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(l) dimer; (2-(diisopropylsilyl)phenyl)di-p-tolylphosphane; In tetrahydrofuran; at 80 ℃; Inert atmosphere;