ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate

Base Information

Chemical Name:ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate
CAS No.:1354438-83-7
Molecular Formula:C₁₄H₁₇Cl₃N₂O₄S
Molecular Weight:415.725
Hs Code.:

Synonyms:ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate

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Chemical Property of ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate

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Technology Process of ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate

There total 5 articles about ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 2163-42-0
2-methyl-1.3-propanediol

: 1354438-71-3
ethyl 2-((N-(2,4,6-trichlorophenyl)sulfamoyl)amino)acetate

: 1354438-83-7
ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/ml200226x

Reference yield:

: C₁₀H₁₁Cl₃N₂O₂S

: 105-36-2
ethyl bromoacetate

: 1354438-83-7
ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2019.126787

Reference yield:

: 634-93-5
2,4,6-trichloroaniline

: 1354438-83-7
ethyl 2-(4-methyl-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 4 h / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3 h / 0 °C

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; 2: Mitsunobu reaction;
DOI:10.1021/ml200226x