C₄₀H₄₉NO₈Si

Base Information

Chemical Name:C₄₀H₄₉NO₈Si
CAS No.:1265173-16-7
Molecular Formula:C₄₀H₄₉NO₈Si
Molecular Weight:699.916
Hs Code.:

C<sub>40</sub>H<sub>49</sub>NO<sub>8</sub>Si

Synonyms:C₄₀H₄₉NO₈Si

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Chemical Property of C₄₀H₄₉NO₈Si

Chemical Property:

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Technology Process of C₄₀H₄₉NO₈Si

There total 27 articles about C₄₀H₄₉NO₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1265173-15-6
C₃₄H₃₉NO₈Si

: 112520-99-7,1177092-71-5
tributyl(cyclohex-2-en-1-yl)stannane

: 1265173-16-7
C₄₀H₄₉NO₈Si

Guidance literature:: tributyl(cyclohex-2-en-1-yl)stannane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

With zinc(II) chloride; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

C₃₄H₃₉NO₈Si; In tetrahydrofuran; hexane; at -78 ℃; for 6h;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-20-3
C₂₂H₂₈O₇S

: 1265173-16-7
C₄₀H₄₉NO₈Si

Guidance literature:: Multi-step reaction with 19 steps

1.1: acetic anhydride; dimethyl sulfoxide / 2 h / 50 °C

2.1: toluene / 4 h / -40 °C

3.1: magnesium / methanol / 2 h / 20 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

5.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

5.2: 0 - 20 °C

6.1: pyridine / dichloromethane / 2 h / 0 °C

7.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

8.1: dichloromethane / 1 h / 0 °C

9.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

10.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

11.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

13.1: scandium tris(trifluoromethanesulfonate) / dichloromethane; water / 20 - 40 °C

14.1: Jones reagent / water; acetone / 0 - 20 °C

15.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 20 °C

16.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

17.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 20 - 60 °C

18.1: pyridine; sodium periodate; osmium(VIII) oxide / water; tert-butyl alcohol / 20 - 50 °C

19.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

19.2: 0.33 h / -78 °C

19.3: 6 h / -78 °C

With pyridine; 2,6-dimethylpyridine; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; Jones reagent; n-butyllithium; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; acetic anhydride; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; mineral oil; tert-butyl alcohol; 4.1: Swern oxidation / 5.2: Horner-Wadsworth-Emmons olefination / 9.1: Overman rearrangement / 15.1: Kraus-Pinnick reaction;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-03-2
C₂₂H₂₆O₇S

: 1265173-16-7
C₄₀H₄₉NO₈Si

Guidance literature:: Multi-step reaction with 18 steps

1.1: toluene / 4 h / -40 °C

2.1: magnesium / methanol / 2 h / 20 °C

3.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

4.2: 0 - 20 °C

5.1: pyridine / dichloromethane / 2 h / 0 °C

6.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

7.1: dichloromethane / 1 h / 0 °C

8.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

9.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

10.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

12.1: scandium tris(trifluoromethanesulfonate) / dichloromethane; water / 20 - 40 °C

13.1: Jones reagent / water; acetone / 0 - 20 °C

14.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 20 °C

15.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

16.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 20 - 60 °C

17.1: pyridine; sodium periodate; osmium(VIII) oxide / water; tert-butyl alcohol / 20 - 50 °C

18.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

18.2: 0.33 h / -78 °C

18.3: 6 h / -78 °C

With pyridine; 2,6-dimethylpyridine; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; Jones reagent; n-butyllithium; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; mineral oil; tert-butyl alcohol; 3.1: Swern oxidation / 4.2: Horner-Wadsworth-Emmons olefination / 8.1: Overman rearrangement / 14.1: Kraus-Pinnick reaction;
DOI:10.1002/asia.201000602