4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid

Base Information

Chemical Name:4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid
CAS No.:910035-25-5
Molecular Formula:C₁₈H₁₉N₂O₉P
Molecular Weight:438.331
Hs Code.:

Synonyms:4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid

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Chemical Property of 4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid

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Technology Process of 4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid

There total 5 articles about 4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910035-13-1
methyl 2-(N-4-nitrobenzyloxycarbonylamino)-4-(diphenylphosphono)butanoate

: 910035-25-5
4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 25h;
DOI:10.1016/j.bmc.2006.05.008

Reference yield:

: 910035-11-9
C₁₃H₁₅Cl₂N₂O₇P

: 910035-25-5
4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 0.79 g / triethylamine / CH₂Cl₂ / 1.67 h / 0 °C

2: NaOH / H₂O; tetrahydrofuran / 25 h / 20 °C

With sodium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmc.2006.05.008

Reference yield:

: 910035-09-5
methyl 2-(N-4-nitrobenzyloxycarbonylamino)-4-phosphonobutanoate

: 910035-25-5
4-(hydroxy-phenoxy-phosphoryl)-2-(4-nitro-benzyloxycarbonylamino)-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; dimethylformamide / CH₂Cl₂ / 2 h / Heating

2: 0.79 g / triethylamine / CH₂Cl₂ / 1.67 h / 0 °C

3: NaOH / H₂O; tetrahydrofuran / 25 h / 20 °C

With sodium hydroxide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmc.2006.05.008