(S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

Base Information

Chemical Name:(S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide
CAS No.:121451-45-4
Molecular Formula:C₂₄H₂₆Cl₂N₂O₂S₂
Molecular Weight:509.521
Hs Code.:

Synonyms:(S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

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Chemical Property of (S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

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Technology Process of (S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

There total 5 articles about (S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 121451-42-1
N-(2-mercaptobenzoyl)-L-prolinol

: 121451-45-4
(S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

Guidance literature:: With thionyl chloride; In benzene; for 1.5h; Heating;
DOI:10.1002/jhet.5570250358

Reference yield: 99.0%

: 19602-82-5
2,2'-dithiodibenzoic acid dichloride

: 35120-33-3
(S)-2-(chloromethyl)pyrrolidine hydrochloride

: 121451-45-4
(S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

Guidance literature:: With triethylamine; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1002/jhet.5570250358

Reference yield: 98.0%

: 121451-41-0
(S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

: 121451-45-4
(S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

Guidance literature:: With thionyl chloride; air; In chloroform; for 2h; Heating; room temperature 1 h, then reflux 2 h;
DOI:10.1002/jhet.5570250358