N⁽¹⁾-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin

Base Information

• Chemical Name: N⁽¹⁾-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin
• CAS No.: 95748-46-2
• Molecular Formula: C₂₄H₃₈N₄O₇
• Molecular Weight: 494.588

Synonyms:N⁽¹⁾-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin

Chemical Property of N⁽¹⁾-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin

Chemical Property:

• Density: 1.211[at 20℃]

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N⁽¹⁾-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin

There total 7 articles about N⁽¹⁾-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(Carbobenzoxyamino)-5-(hydroxyamino)pentane (91905-05-4) → N(1)-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin (95748-46-2)

Guidance literature:

Multi-step reaction with 4 steps

1: Py

2: acetic anhydride / 5 h / 95 - 100 °C

3: (i) NaOMe, MeOH, (ii) /BRN= 898057/, THF

4: (i) aq. NH₄Cl, Zn, EtOH, (ii) /BRN= 385737/, Py

With pyridine; In acetic anhydride;

DOI:10.1002/hlca.19620450228

Reference yield:

1-Carbobenzoxyamino-5-nitro-pentan (92034-20-3) → N(1)-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin (95748-46-2)

Guidance literature:

Multi-step reaction with 5 steps

1: aq. NH₄Cl, Zn / ethanol

2: Py

3: acetic anhydride / 5 h / 95 - 100 °C

4: (i) NaOMe, MeOH, (ii) /BRN= 898057/, THF

5: (i) aq. NH₄Cl, Zn, EtOH, (ii) /BRN= 385737/, Py

With pyridine; ammonium chloride; zinc; In ethanol; acetic anhydride;

DOI:10.1002/hlca.19620450228

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → N(1)-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin (95748-46-2)

Guidance literature:

Multi-step reaction with 6 steps

1: aq. NaOH

2: aq. NH₄Cl, Zn / ethanol

3: Py

4: acetic anhydride / 5 h / 95 - 100 °C

5: (i) NaOMe, MeOH, (ii) /BRN= 898057/, THF

6: (i) aq. NH₄Cl, Zn, EtOH, (ii) /BRN= 385737/, Py

With pyridine; sodium hydroxide; ammonium chloride; zinc; In ethanol; acetic anhydride;

DOI:10.1002/hlca.19620450228

upstream raw materials:

1-Carbobenzoxyamino-6-hydroxy-16-nitro-7,10-dioxo-6,11-diaza-hexadecan

acetic anhydride

1-(Carbobenzoxyamino)-5-(hydroxyamino)pentane

1-Carbobenzoxyamino-5-nitro-pentan

Downstream raw materials:

benzoylamide deferoxamine

1-Carbobenzoxyamino-6,17-dihydroxy-7,10,18,21-tetraoxy-27-(N-acetyl-hydroxyamino)-6,11,17,22-tetraaza-hepteikosan

deferoxamine

1,5-diaminopentane

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