(N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

Base Information

Chemical Name:(N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>
CAS No.:87589-44-4
Molecular Formula:C₃₀H₅₁N₃O₉
Molecular Weight:597.75
Hs Code.:

(N,N-dimethylcarbamoyl)methylene bis<trans-4<<(tert-butoxycarbonyl)amino>methyl>cyclohexanecarboxylate>

Synonyms:(N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

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Chemical Property of (N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

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Technology Process of (N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

There total 4 articles about (N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66178-47-0
dibromo-acetic acid dimethylamide

: 27687-14-5
trans 4-(tert-butyloxycarbonylamino)methylcyclohexanecarboxylic acid

: 87589-44-4
(N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 84h; Yield given;
DOI:10.1021/jm00154a004

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 87589-44-4
(N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: Et₃N / dimethylformamide / 84 h / 50 °C

With sodium hydroxide; triethylamine; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm00154a004

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 87589-44-4
(N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: Et₃N / dimethylformamide / 84 h / 50 °C

With sodium hydroxide; triethylamine; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm00154a004