2-benzylthio-4--5-thiazolone

Base Information

• Chemical Name: 2-benzylthio-4--5-thiazolone
• CAS No.: 100711-02-2
• Molecular Formula: C₁₄H₁₅NO₂S₂
• Molecular Weight: 293.411

Synonyms:2-benzylthio-4--5-thiazolone

Chemical Property of 2-benzylthio-4--5-thiazolone

Chemical Property:

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Technology Process of 2-benzylthio-4--5-thiazolone

There total 4 articles about 2-benzylthio-4--5-thiazolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

benzyl bromide (100-39-0) + 4-<(Z)-1-ethoxyethylidene>-2-thiono-5-thiazolinone → 2-benzylthio-4--5-thiazolone (100711-02-2)

Guidance literature:

With potassium carbonate; In acetone; for 0.5h;

Reference yield: 67.0%

2-(((benzylthio)carbonothioyl)amino)acetic acid (4596-57-0) + Triethyl orthoacetate (78-39-7) → 2-benzylthio-4--5-thiazolone (100711-02-2) + 2-benzylthio-4--5-thiazolone (100711-02-2)

Guidance literature:

With o-toluenesulfonic acid; In acetic anhydride; for 0.166667h; Yield given;

Reference yield: 67.0%

2-(((benzylthio)carbonothioyl)amino)acetic acid (4596-57-0) + Triethyl orthoacetate (78-39-7) → 2-benzylthio-4--5-thiazolone (100711-02-2) + 2-benzylthio-4--5-thiazolone (100711-02-2)

Guidance literature:

With o-toluenesulfonic acid; In acetic anhydride; for 0.166667h; Yield given;

upstream raw materials:

2-(((benzylthio)carbonothioyl)amino)acetic acid

Triethyl orthoacetate

benzyl bromide

Downstream raw materials:

4-[1-ethoxy-4-(3-ethyl-3H-benzoxazol-2-ylidene)-but-2-enylidene]-2-benzylmercapto-4H-thiazol-5-one

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