(S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane

Base Information

Chemical Name:(S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane
CAS No.:389085-90-9
Molecular Formula:C₂₆H₄₄O₄S₂Si
Molecular Weight:512.85
Hs Code.:

Synonyms:(S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane

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Chemical Property of (S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane

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Technology Process of (S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane

There total 5 articles about (S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 994-30-9
triethylsilyl chloride

: 389086-05-9
(S)-4-(2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-1,3-dithian-2-yl)-1-butanol

: 389085-90-9
(S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/S0040-4020(02)01379-0

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 389085-90-9
(S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 6 h / 20 °C

2: 98 percent / imidazole / CH₂Cl₂ / 2 h / 0 - 20 °C

With 1H-imidazole; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1016/S0040-4020(02)01379-0

Reference yield:

: 389086-04-8
(S)-4-[2-(4-hydroxybutyl)-1,3-dithian-2-yl]-butane-1,2-diol

: 389085-90-9
(S)-2-{2-[2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]ethyl}-2-[4-(triethylsilyloxy)butyl]-1,3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 6 h / 20 °C

2: 98 percent / imidazole / CH₂Cl₂ / 2 h / 0 - 20 °C

With 1H-imidazole; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1016/S0040-4020(02)01379-0