Technology Process of C16H22O2S
There total 4 articles about C16H22O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Lawessons reagent;
In
xylenes;
for 3h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate; tetrabutyl-ammonium chloride / palladium diacetate / N,N-dimethyl-formamide / 1 h / 70 °C
1.2: 20 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 2585.81 Torr
3.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C
4.1: Lawessons reagent / xylenes / 3 h / Reflux
With
Lawessons reagent; tetrabutyl-ammonium chloride; hydrogen; potassium carbonate;
palladium 10% on activated carbon; palladium diacetate;
In
methanol; N,N-dimethyl-formamide; xylenes;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen / palladium 10% on activated carbon / methanol / 2585.81 Torr
2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C
3: Lawessons reagent / xylenes / 3 h / Reflux
With
Lawessons reagent; hydrogen; potassium carbonate;
palladium 10% on activated carbon;
In
methanol; N,N-dimethyl-formamide; xylenes;