methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate

Base Information

Chemical Name:methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate
CAS No.:1263291-80-0
Molecular Formula:C₂HF₃O₂*C₁₅H₁₇F₂NO₃
Molecular Weight:411.326
Hs Code.:

Synonyms:methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate

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Chemical Property of methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate

Chemical Property:

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Technology Process of methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate

There total 1 articles about methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60421-23-0
cycloleucine methyl ester hydrochloride

: 76-05-1
trifluoroacetic acid

: 1263291-80-0
methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate

Guidance literature:: 2-bromo-1-(3,5-difluorophenyl)ethanone; cycloleucine methyl ester hydrochloride; With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

trifluoroacetic acid; In water; acetonitrile; HPLC with reversed phase C₁₈ column;

Reference yield:

: 1263291-80-0
methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate

: 623-33-6
glycine ethyl ester hydrochloride

: 957121-89-0
ethyl [(8R)-8-(3,5-difluorophenyl)-10-oxo-6,9-diazaspiro[4.5]dec-9-yl]acetate

: ethyl [(8S)-8-(3,5-difluorophenyl)-10-oxo-6,9-diazaspiro[4.5]dec-9-yl]acetate

Guidance literature:: methyl 1-{[2-(3,5-difluorophenyl)-2-oxoethyl]amino}cyclopentanecarboxylate trifluoroacetate; glycine ethyl ester hydrochloride; With acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; at 20 ℃; for 0.166667h;

With sodium cyanoborohydride; In methanol; at 60 ℃; for 72h;