Technology Process of N-(2-(β-ammonioethyl)phenyl)anthranilat
There total 10 articles about N-(2-(β-ammonioethyl)phenyl)anthranilat which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
for 65h;
under 2100.17 Torr;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 68 percent / K2CO3 / Cu; CuI / dibutyl ether / 22 h / 175 °C
2: 99 percent / aq. HCl / acetone / 1.5 h / 30 °C
3: 99 percent / NaBH4 / diethyl ether / Heating
4: SOCl2; pyridine / diethyl ether / 1 h
5: dimethylsulfoxide / 1 h / 40 °C
6: 84 percent / BH3*THF / tetrahydrofuran / 1.5 h / Heating
7: 70 percent / K2CO3 / CH2Cl2 / 60 h / 20 °C
8: 96 percent / NaOH / ethanol; H2O / 60 h / 20 °C
9: 98 percent / H2 / 10 percent Pd-C / ethanol / 65 h / 2100.17 Torr
With
pyridine; hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; borane-THF; hydrogen; potassium carbonate;
palladium on activated charcoal; copper(l) iodide; copper;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; dibutyl ether; water; dimethyl sulfoxide; acetone;
1: Substitution / 2: Ring cleavage / 3: Reduction / 4: Chlorination / 5: Substitution / 6: Reduction / 7: Carboxylation / 8: Hydrolysis / 9: Hydrogenolysis;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 68 percent / K2CO3 / Cu; CuI / dibutyl ether / 22 h / 175 °C
2: 99 percent / aq. HCl / acetone / 1.5 h / 30 °C
3: 99 percent / NaBH4 / diethyl ether / Heating
4: SOCl2; pyridine / diethyl ether / 1 h
5: dimethylsulfoxide / 1 h / 40 °C
6: 84 percent / BH3*THF / tetrahydrofuran / 1.5 h / Heating
7: 70 percent / K2CO3 / CH2Cl2 / 60 h / 20 °C
8: 96 percent / NaOH / ethanol; H2O / 60 h / 20 °C
9: 98 percent / H2 / 10 percent Pd-C / ethanol / 65 h / 2100.17 Torr
With
pyridine; hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; borane-THF; hydrogen; potassium carbonate;
palladium on activated charcoal; copper(l) iodide; copper;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; dibutyl ether; water; dimethyl sulfoxide; acetone;
1: Substitution / 2: Ring cleavage / 3: Reduction / 4: Chlorination / 5: Substitution / 6: Reduction / 7: Carboxylation / 8: Hydrolysis / 9: Hydrogenolysis;
