H-Leu-Val-Phe-OMe

Base Information

Chemical Name:H-Leu-Val-Phe-OMe
CAS No.:52828-91-8
Molecular Formula:C₂₁H₃₃N₃O₄
Molecular Weight:391.511
Hs Code.:

Synonyms:H-Leu-Val-Phe-OMe

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-Leu-Val-Phe-OMe

Chemical Property:

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Technology Process of H-Leu-Val-Phe-OMe

There total 12 articles about H-Leu-Val-Phe-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 78123-60-1
methyl (S)-2-<<(tert-butoxycarbonyl)-(S)-leucinyl-(S)-valinyl>amino>-3-phenylpropanoate

: 52828-91-8
H-Leu-Val-Phe-OMe

Guidance literature:: methyl (S)-2-<<(tert-butoxycarbonyl)-(S)-leucinyl-(S)-valinyl>amino>-3-phenylpropanoate; With trifluoroacetic acid; at 0 - 20 ℃;

With sodium carbonate; In water; ethyl acetate;
DOI:10.1039/c3cc43371d

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 52828-91-8
H-Leu-Val-Phe-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*BF₄^(1-); diisopropylethylamine / CH₂Cl₂ / 20 °C

2: 100 percent / trifluoroacetic acid; anisole / CH₂Cl₂

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*BF₄^(1-); diisopropylethylamine / CH₂Cl₂ / 20 °C

4: trifluoroacetic acid; anisole / CH₂Cl₂

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2006.04.031

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 52828-91-8
H-Leu-Val-Phe-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*BF₄^(1-); diisopropylethylamine / CH₂Cl₂ / 20 °C

2: 100 percent / trifluoroacetic acid; anisole / CH₂Cl₂

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*BF₄^(1-); diisopropylethylamine / CH₂Cl₂ / 20 °C

4: trifluoroacetic acid; anisole / CH₂Cl₂

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2006.04.031