N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide

Base Information

Chemical Name:N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide
CAS No.:1298055-82-9
Molecular Formula:C₂₈H₃₃N₃O₂
Molecular Weight:443.589
Hs Code.:

Synonyms:N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide

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Chemical Property of N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide

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Technology Process of N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide

There total 5 articles about N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1298055-72-7
N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-chloroacetamide

: 109-89-7
diethylamine

: 1298055-82-9
N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide

Guidance literature:: In propan-1-ol; for 8h; Reflux;
DOI:10.1016/j.ejmech.2011.02.019

Reference yield:

: 1298055-70-5
(4-((benzyl(methyl)amino)methyl)phenyl)(4-nitrophenyl)methanone

: 1298055-82-9
N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 10% Pd/CaCO3; hydrogen / tetrahydrofuran / 20 °C

2: acetonitrile / 6 h / Reflux

3: propan-1-ol / 8 h / Reflux

With 10% Pd/CaCO3; hydrogen; In tetrahydrofuran; propan-1-ol; acetonitrile;
DOI:10.1016/j.ejmech.2011.02.019

Reference yield:

: 5350-47-0
(4-methylphenyl)(4-nitrophenyl)methanone

: 1298055-82-9
N-(4-{4-[(benzylmethylamino)methyl]benzoyl}phenyl)-2-diethylaminoacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 6 h / 60 °C

2: triethylamine / toluene / 12 h / Reflux

3: 10% Pd/CaCO3; hydrogen / tetrahydrofuran / 20 °C

4: acetonitrile / 6 h / Reflux

5: propan-1-ol / 8 h / Reflux

With N-Bromosuccinimide; 10% Pd/CaCO3; hydrogen; triethylamine; dibenzoyl peroxide; In tetrahydrofuran; propan-1-ol; tetrachloromethane; toluene; acetonitrile;
DOI:10.1016/j.ejmech.2011.02.019