C₁₉H₁₆ClNO₃

Base Information

Chemical Name:C₁₉H₁₆ClNO₃
CAS No.:1278540-54-7
Molecular Formula:C₁₉H₁₆ClNO₃
Molecular Weight:341.794
Hs Code.:

C<sub>19</sub>H<sub>16</sub>ClNO<sub>3</sub>

Synonyms:C₁₉H₁₆ClNO₃

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Chemical Property of C₁₉H₁₆ClNO₃

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Technology Process of C₁₉H₁₆ClNO₃

There total 3 articles about C₁₉H₁₆ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1278540-59-2
C₂₆H₂₂ClNO₃

: 1278540-54-7
C₁₉H₁₆ClNO₃

Guidance literature:: With 10% Pd/C; hydrogen; In ethyl acetate; at 20 ℃; for 4h; under 760.051 Torr;
DOI:10.1021/jm301084z

Reference yield:

: 1278540-62-7
C₁₉H₁₉NO₂

: 122-01-0
4-chloro-benzoyl chloride

: 1278540-54-7
C₁₉H₁₆ClNO₃

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / -78 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate

With palladium 10% on activated carbon; potassium tert-butylate; hydrogen; In tetrahydrofuran; ethyl acetate;
DOI:10.1021/ml100292y

Reference yield:

: 1192805-45-0
N-p-toluenesulfonyl-2-ethylindole

: 1278540-54-7
C₁₉H₁₆ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / methanol / 4 h / Reflux

2.1: n-butyllithium; zinc(II) chloride / tetrahydrofuran; hexane / 1.83 h / 0 - 20 °C

2.2: 18 h

3.1: potassium tert-butylate / tetrahydrofuran / 1 h / -40 °C

3.2: 3 h

4.1: 10% Pd/C; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr

With n-butyllithium; 10% Pd/C; potassium tert-butylate; hydrogen; potassium hydroxide; zinc(II) chloride; In tetrahydrofuran; methanol; hexane; ethyl acetate;
DOI:10.1021/jm301084z