Technology Process of C72H91N9O17S
There total 20 articles about C72H91N9O17S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 86 percent / DCC, HOBt
2: H2 / Pd/C
4: LiOH
5: CsCO3
6: p-TsOH / acetonitrile; CH2Cl2
7: Et3N, DMAP / CH2Cl2
8: p-TsOH / acetonitrile; CH2Cl2
9: BOP, DMAP / CH2Cl2 / Ambient temperature
10: p-TsOH / acetonitrile; CH2Cl2
11: BOP, DMAP / CH2Cl2 / Ambient temperature
With
dmap; lithium hydroxide; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; toluene-4-sulfonic acid; triethylamine; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja00042a053
- Guidance literature:
-
Multi-step reaction with 10 steps
1: H2 / Pd/C
3: LiOH
4: CsCO3
5: p-TsOH / acetonitrile; CH2Cl2
6: Et3N, DMAP / CH2Cl2
7: p-TsOH / acetonitrile; CH2Cl2
8: BOP, DMAP / CH2Cl2 / Ambient temperature
9: p-TsOH / acetonitrile; CH2Cl2
10: BOP, DMAP / CH2Cl2 / Ambient temperature
With
dmap; lithium hydroxide; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; toluene-4-sulfonic acid; triethylamine;
palladium on activated charcoal;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja00042a053
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / DMAP
2: LiAlH4 / tetrahydrofuran
3: 1.) n-BuLi, 2.) HgO, HgCl2, H2O, 3.) aq. LiOH
4: BOP, DMAP / CH2Cl2 / Ambient temperature
With
dmap; lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; mercury dichloride; mercury(II) oxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00042a053