Boranamine, N,N-dimethyl-1,1-bis(1-methylethyl)-

Base Information

• Chemical Name: Boranamine, N,N-dimethyl-1,1-bis(1-methylethyl)-
• CAS No.: 90324-59-7
• Molecular Formula: C₈H₂₀BN
• Molecular Weight: 141.064
• DSSTox Substance ID: DTXSID801239630
• Mol file: 90324-59-7.mol

Synonyms:90324-59-7;Boranamine, N,N-dimethyl-1,1-bis(1-methylethyl)-;DTXSID801239630

Chemical Property of Boranamine, N,N-dimethyl-1,1-bis(1-methylethyl)-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 141.1688798
• Heavy Atom Count: 10
• Complexity: 81.3

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: B(C(C)C)(C(C)C)N(C)C

Technology Process of Boranamine, N,N-dimethyl-1,1-bis(1-methylethyl)-

There total 1 articles about Boranamine, N,N-dimethyl-1,1-bis(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

isopropyllithium (1888-75-1) + 1-dimethylamino-1,3-dioxa-2-boracycloheptane (17739-06-9) → (dimethylamino)diisopropylborane (90324-59-7) + triisopropylborane (1776-66-5) + tris(dimethylamino)borane (4375-83-1)

Guidance literature:

In hexane; (N2); without moisture; added soln. of Li-compound to soln. of B-compound at -70°C under stirring; warmed at room temp.; refluxed for 1 h; filtered; washed with hexane; evapd. in vac.; distd. at 60°C/29 Torr; (11)B NMR;

Reference yield:

(dimethylamino)diisopropylborane (90324-59-7) → (diphenylamino)diisopropylborane (106367-67-3)

Guidance literature:

Multi-step reaction with 4 steps

1: CH₃OH / pentane

3: BH₃ / tetrahydrofuran

4: hexane

With CH₃OH; BH₃; In tetrahydrofuran; hexane; pentane;

Reference yield:

(dimethylamino)diisopropylborane (90324-59-7) → triisopropylborane (1776-66-5)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₃OH / pentane

With CH₃OH; In pentane;

upstream raw materials:

isopropyllithium

1-dimethylamino-1,3-dioxa-2-boracycloheptane

Downstream raw materials:

triisopropylborane

(diphenylamino)diisopropylborane