[4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester

Base Information

Chemical Name:[4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester
CAS No.:869337-35-9
Molecular Formula:C₁₇H₂₈BrN₂O₄P
Molecular Weight:435.298
Hs Code.:

Synonyms:[4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester

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Chemical Property of [4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester

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Technology Process of [4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester

There total 3 articles about [4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 869337-28-0
N-DIPP-5-aminopentanoic acid

: 615-36-1
2-bromoaniline

: 869337-35-9
[4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester

Guidance literature:: With pyridine; diphenyl phosphite; at 20 ℃; for 2h;
DOI:10.1021/ol052126c

Reference yield:

: 1809-20-7
diisopropyl hydrogenphosphonate

: 869337-35-9
[4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Et₃N / CCl₄; H₂O; ethanol / 0 - 20 °C

2: 85 percent / diphenyl phosphite; pyridine / 2 h / 20 °C

With pyridine; diphenyl phosphite; triethylamine; In tetrachloromethane; ethanol; water;
DOI:10.1021/ol052126c

Reference yield:

: 660-88-8
5-aminopentanoic acid

: 869337-35-9
[4-(2-bromo-phenylcarbamoyl)-butyl]-phosphoramidic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Et₃N / CCl₄; H₂O; ethanol / 0 - 20 °C

2: 85 percent / diphenyl phosphite; pyridine / 2 h / 20 °C

With pyridine; diphenyl phosphite; triethylamine; In tetrachloromethane; ethanol; water;
DOI:10.1021/ol052126c