3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione

Base Information

Chemical Name:3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione
CAS No.:1308788-89-7
Molecular Formula:C₁₈H₁₇BrN₂O₂
Molecular Weight:373.249
Hs Code.:

Synonyms:3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione

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Chemical Property of 3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione

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Technology Process of 3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione

There total 5 articles about 3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 201230-82-2
carbon monoxide

: 1308788-43-3
3-(3-bromophenyl)-2,2-dimethyl-N-(pyridin-2-ylmethyl)propanamide

: 1308788-89-7
3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione

Guidance literature:: With dodecacarbonyl-triangulo-triruthenium; ethene; water; In toluene; at 160 ℃; for 120h; under 12920.9 Torr; regioselective reaction; Autoclave;
DOI:10.1021/ja2001709

Reference yield:

: 3-(3-bromo-phenyl)-2,2-dimethyl-propionyl chloride

: 1308788-89-7
3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0 - 20 °C / Inert atmosphere

2: dodecacarbonyl-triangulo-triruthenium; ethene; water / toluene / 120 h / 160 °C / 12920.9 Torr / Autoclave

With dodecacarbonyl-triangulo-triruthenium; ethene; water; In dichloromethane; toluene;
DOI:10.1021/ja2001709

Reference yield:

: 926625-06-1
3-(3-bromophenyl)-2,2-dimethylpropionic acid

: 1308788-89-7
3-(3-bromobenzyl)-3-methyl-1-(pyridin-2-ylmethyl)pyrrolidine-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / 85 °C / Inert atmosphere

2: dichloromethane / 0 - 20 °C / Inert atmosphere

3: dodecacarbonyl-triangulo-triruthenium; ethene; water / toluene / 120 h / 160 °C / 12920.9 Torr / Autoclave

With thionyl chloride; dodecacarbonyl-triangulo-triruthenium; ethene; water; In dichloromethane; toluene;
DOI:10.1021/ja2001709