1,1-biscyclohexanemethanol

Base Information

• Chemical Name: 1,1-biscyclohexanemethanol
• CAS No.: 155397-15-2
• Molecular Formula: C₂₃H₃₄OSi₂
• Molecular Weight: 382.693

Synonyms:1,1-biscyclohexanemethanol

Chemical Property of 1,1-biscyclohexanemethanol

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Technology Process of 1,1-biscyclohexanemethanol

There total 3 articles about 1,1-biscyclohexanemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

dimethyl(phenyl)silyllithium (3839-31-4) + cyclohexanylcarbonyl chloride (2719-27-9) → 1,1-biscyclohexanemethanol (155397-15-2)

Guidance literature:

In tetrahydrofuran; toluene; at -78 ℃;

DOI:10.1002/1522-2675(200210)85:10<3349::AID-HLCA3349>3.0.CO;2-K

Reference yield: 81.0%

phenyl cyclohexanecarboxylate (3954-12-9) + dimethyl(phenyl)silyllithium (3839-31-4) → 1,1-biscyclohexanemethanol (155397-15-2)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 3h;

Reference yield: 63.0%

methyl cyclohexylcarboxylate (4630-82-4) + dimethyl(phenyl)silyllithium (3839-31-4) → 1-dimethyl(methoxy)silyl-1-phenylcyclohexylmethanol + 1,1-biscyclohexanemethanol (155397-15-2)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 3h;

upstream raw materials:

methyl cyclohexylcarboxylate

dimethyl(phenyl)silyllithium

phenyl cyclohexanecarboxylate

cyclohexanylcarbonyl chloride

Downstream raw materials:

1-cyclohexyl-1-[dimethyl(phenyl)silyl]-1-[dimethyl(phenyl)silyloxy]-3-methylbutane

1-cyclohexyl-2-methylpropan-1-one

1-cyclohexyl-2-methylpropan-1-ol

Cyclohexyl 2-methylpropyl ketone

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