4-acetyl-N-methyl-N-phenylbenzamide

Base Information

Chemical Name:4-acetyl-N-methyl-N-phenylbenzamide
CAS No.:1415466-25-9
Molecular Formula:C₁₆H₁₅NO₂
Molecular Weight:253.301
Hs Code.:

Synonyms:4-acetyl-N-methyl-N-phenylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetyl-N-methyl-N-phenylbenzamide

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Technology Process of 4-acetyl-N-methyl-N-phenylbenzamide

There total 2 articles about 4-acetyl-N-methyl-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 586-89-0
4-acetyl-benzoic acid

: 100-61-8
N-methylaniline

: 1415466-25-9
4-acetyl-N-methyl-N-phenylbenzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 40 ℃; for 1h;

Reference yield: 81.0%

: 13329-40-3
4-Iodoacetophenone

: 201230-82-2
carbon monoxide

: 100-61-8
N-methylaniline

: 1415466-25-9
4-acetyl-N-methyl-N-phenylbenzamide

Guidance literature:: 4-Iodoacetophenone; N-methylaniline; With sodium carbonate; In water; for 0.166667h; Autoclave;

carbon monoxide; In water; at 100 ℃; for 8h; under 5171.62 Torr; Autoclave;
DOI:10.1016/j.cattod.2012.03.039

Reference yield: 68.0%

: 1415466-25-9
4-acetyl-N-methyl-N-phenylbenzamide

: 9-[3-(4-methoxy-phenyl)-propyl]-9-bora-bicyclo[3.3.1]nonane

: 1-(4-acetylphenyl)-4-(4-methoxyphenyl)butan-1-one

Guidance literature:: 4-acetyl-N-methyl-N-phenylbenzamide; With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium carbonate; lithium chloride; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In di-isopropyl ether; at 20 ℃; for 0.0833333h; Sealed tube; Glovebox; Inert atmosphere;

9-[3-(4-methoxy-phenyl)-propyl]-9-bora-bicyclo[3.3.1]nonane; In di-isopropyl ether; at 90 ℃; for 36h; chemoselective reaction; Sealed tube; Glovebox; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01021