2,2',7,7'-tetraiodo-9-fluorenyl dimer

Base Information

Chemical Name:2,2',7,7'-tetraiodo-9-fluorenyl dimer
CAS No.:39168-56-4
Molecular Formula:C₂₆H₁₄I₄
Molecular Weight:834.015
Hs Code.:

Synonyms:2,2',7,7'-tetraiodo-9-fluorenyl dimer

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Chemical Property of 2,2',7,7'-tetraiodo-9-fluorenyl dimer

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Technology Process of 2,2',7,7'-tetraiodo-9-fluorenyl dimer

There total 2 articles about 2,2',7,7'-tetraiodo-9-fluorenyl dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 67-56-1
methanol

: 94721-46-7
9-diazo-2,7-diiodo-9H-fluorene

: 16218-28-3
2,7-diiodofluorene

: 39168-56-4
2,2',7,7'-tetraiodo-9-fluorenyl dimer

: 2,7-diiodofluorenyl methyl ether

Guidance literature:: With 11H-Benzo[b]fluoren-11-one; In acetonitrile; for 0.833333h; Irradiation;
DOI:10.1021/ja00250a039

Reference yield:

: 2523-42-4
2-iodo-9H-fluorene

: 39168-56-4
2,2',7,7'-tetraiodo-9-fluorenyl dimer

Guidance literature:: Multi-step reaction with 4 steps

2: NBS

3: NaOH / methanol; butan-2-one

4: NaOEt / ethanol

With sodium hydroxide; N-Bromosuccinimide; sodium ethanolate; In methanol; ethanol; butanone;
DOI:10.1246/bcsj.45.3196