2--4-phenyl-1,3-dioxolane

Base Information

• Chemical Name: 2--4-phenyl-1,3-dioxolane
• CAS No.: 120235-63-4
• Molecular Formula: C₁₅H₁₂FNO₂
• Molecular Weight: 257.264
• Mol file: 120235-63-4.mol

Synonyms:2--4-phenyl-1,3-dioxolane

Chemical Property of 2--4-phenyl-1,3-dioxolane

Chemical Property:

Purity/Quality:

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• Hazard Codes: 

MSDS Files:

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Technology Process of 2--4-phenyl-1,3-dioxolane

There total 1 articles about 2--4-phenyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylethane 1,2-diol (93-56-1) + 4-Fluor-phenylisocyaniddichlorid (14210-24-3) → 2--4-phenyl-1,3-dioxolane (120235-63-4)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) dioxane, reflux, 2 h; 2.) dioxane, reflux, 2 h;

DOI:10.1039/P29880001653

Reference yield: 30.0%

2--4-phenyl-1,3-dioxolane (120235-63-4) → (4-Fluoro-phenyl)-carbamic acid 2-hydroxy-2-phenyl-ethyl ester + (4-Fluoro-phenyl)-carbamic acid 2-hydroxy-1-phenyl-ethyl ester

Guidance literature:

In water; at 60 ℃; Rate constant; Mechanism; hydrolysis at pH=11,3, 0.8M KCl;

DOI:10.1039/P29880001653

Reference yield:

2--4-phenyl-1,3-dioxolane (120235-63-4) → 4-Phenyl-1,3-dioxolan-2-one (4427-92-3) + 4-fluoroaniline (371-40-4)

Guidance literature:

In water; at 60 ℃; Rate constant; Mechanism; hydrolysis at pH<6, 0.8M KCl;

DOI:10.1039/P29880001653

upstream raw materials:

phenylethane 1,2-diol

4-Fluor-phenylisocyaniddichlorid

Downstream raw materials:

4-Phenyl-1,3-dioxolan-2-one

4-fluoroaniline