tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate

Base Information

Chemical Name:tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate
CAS No.:1309477-56-2
Molecular Formula:C₁₉H₃₁O₈P
Molecular Weight:418.424
Hs Code.:

Synonyms:tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate

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Technology Process of tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate

There total 1 articles about tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1309477-63-1
C₁₇H₂₆O₅

: 121-45-9
phosphorous acid trimethyl ester

: 1309477-56-2
tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate

Guidance literature:: phosphorous acid trimethyl ester; With bromine; In dichloromethane;

C₁₇H₂₆O₅; With pyridine; dmap; In dichloromethane; at -50 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol200991x

Reference yield: 57.0%

: 1309477-56-2
tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate

: tert-butyl 2-(benzyloxymethoxy)cyclopropanecarboxylate

Guidance literature:: tert-butyl 4-(benzyloxymethoxy)-3-((dimethoxyphosphoryloxy)methyl)butanoate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.366667h; Inert atmosphere;

With acetyl chloride; In tetrahydrofuran; at -78 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol200991x