(1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate

Base Information

Chemical Name:(1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate
CAS No.:1290137-23-3
Molecular Formula:C₁₄H₂₀O₆S
Molecular Weight:316.375
Hs Code.:

Synonyms:(1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate

Suppliers and Price of (1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate

Chemical Property:

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Technology Process of (1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate

There total 2 articles about (1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1290137-22-2
C₁₄H₁₈O₄S

: 1290137-23-3
(1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate

: C₁₄H₂₀O₆S

Guidance literature:: With AD-mix β; In water; tert-butyl alcohol; at 0 ℃; for 12h; optical yield given as %de;
DOI:10.1002/ejoc.201001473

Reference yield:

: 110567-21-0
(1S,2R)-2-(benzyloxymethyl)-1-hydroxy-3-cyclopentene

: 1290137-23-3
(1S,2S,3S,4R)-2-(benzyloxymethyl)-3,4-dihydroxycyclopentyl methanesulfonate

: C₁₄H₂₀O₆S

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h

2: AD-mix β / water; tert-butyl alcohol / 12 h / 0 °C

With triethylamine; In tetrahydrofuran; water; tert-butyl alcohol; 2: Sharpless dihydroxylation;
DOI:10.1002/ejoc.201001473