tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate

Base Information

Chemical Name:tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate
CAS No.:1593268-06-4
Molecular Formula:C₂₃H₂₁NO₄
Molecular Weight:376.413
Hs Code.:

tert-butyl 3-(3-(4-methoxyphenyl)(1-<SUP>13</SUP>C)prop-2-ynoyl)-1H-indole-1-carboxylate

Synonyms:tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate

Suppliers and Price of tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate

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Technology Process of tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate

There total 2 articles about tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 143259-56-7
3-bromoindole-1-carboxylic acid tert-butyl ester

: 1641-69-6
[13C]Carbon monoxide

: 768-60-5
4-methoxyphenylacetylen

: 1593268-06-4
tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate

Guidance literature:: With triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium dichloride; In 1,4-dioxane; at 80 ℃; for 16h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.5b01250

Reference yield:

: 143259-56-7
3-bromoindole-1-carboxylic acid tert-butyl ester

: 1072315-89-9
9-methylfluorene-9-([⁽¹³⁾C]-carbonyl) chloride

: 768-60-5
4-methoxyphenylacetylen

: 1593268-06-4
tert-butyl 3-(3-(4-methoxyphenyl)(1-¹³C)prop-2-ynoyl)-1H-indole-1-carboxylate

Guidance literature:: With dichloro(1,5-cyclooctadiene)palladium(II); N-Methyldicyclohexylamine; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate; In 1,4-dioxane; at 80 ℃; for 16h; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1021/ol5007289