triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide

Base Information

Chemical Name:triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide
CAS No.:107769-71-1
Molecular Formula:Br*C₃₀H₂₈N₂O₂P
Molecular Weight:559.442
Hs Code.:

Synonyms:triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide

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Technology Process of triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide

There total 2 articles about triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2091-46-5
triphenyl(prop-2-ynyl)phosphonium bromide

: 23102-11-6
methyl α-hydrazonophenylacetate

: 107769-71-1
triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide

Guidance literature:: In dichloromethane; for 4h; Heating;
DOI:10.1021/jo00385a029

Reference yield:

: 15206-55-0
methyl 2-oxo-2-phenylacetate

: 107769-71-1
triphenyl<2-((phenyl(methoxycarbonyl)methylene)hydrazono)propyl>phosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / aq. hydrazine, aq. HCl / methanol / 96 h / Ambient temperature

2: 75 percent / CH₂Cl₂ / 4 h / Heating

With hydrogenchloride; hydrazine hydrate; In methanol; dichloromethane;
DOI:10.1021/jo00385a029