Technology Process of C14H18O8S
There total 5 articles about C14H18O8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ruthenium trichloride; sodium periodate;
In
water; acetonitrile;
at 0 ℃;
for 0.5h;
DOI:10.1021/ol300293a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2: sodium periodate; ruthenium trichloride / water; acetonitrile / 0.5 h / 0 °C
With
ruthenium trichloride; sodium periodate; thionyl chloride; triethylamine;
In
dichloromethane; water; acetonitrile;
DOI:10.1021/ol300293a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
1.2: 4 h / -78 °C / Inert atmosphere
1.3: -78 - 20 °C / Inert atmosphere
2.1: AD-mix-α; methanesulfonamide; water / tert-butyl alcohol / 96 h / -1 °C
3.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
4.1: sodium periodate; ruthenium trichloride / water; acetonitrile / 0.5 h / 0 °C
With
ruthenium trichloride; sodium periodate; copper(l) iodide; thionyl chloride; methanesulfonamide; AD-mix-α; water; triethylamine;
In
tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol;
1.2: Michael addition / 2.1: Sharpless dihydroxylation;
DOI:10.1021/ol300293a
