2-Methoxy-5-vinylpyrimidine

Base Information

Chemical Name:2-Methoxy-5-vinylpyrimidine
CAS No.:120717-41-1
Molecular Formula:C₇H₈N₂O
Molecular Weight:136.153
Hs Code.:
European Community (EC) Number:968-346-3
Mol file:120717-41-1.mol

Synonyms:120717-41-1;Pyrimidine, 5-ethenyl-2-methoxy- (9CI);5-ETHENYL-2-METHOXYPYRIMIDINE;2-Methoxy-5-vinylpyrimidine;SCHEMBL2870003;LIOOINKSXDJULD-UHFFFAOYSA-N

Suppliers and Price of 2-Methoxy-5-vinylpyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Methoxy-5-vinylpyrimidine

Chemical Property:

Boiling Point:30 °C (0.01 mmHg)
PSA：35.01000
LogP:1.12820
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:136.063662883
Heavy Atom Count:10
Complexity:108

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=NC=C(C=N1)C=C

Technology Process of 2-Methoxy-5-vinylpyrimidine

There total 3 articles about 2-Methoxy-5-vinylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 108-05-4,9003-20-7
vinyl acetate

: 14001-66-2
5-bromo-2-methoxypyrimidine

: 120717-41-1
2-methoxy-5-vinylpyrimidine

Guidance literature:: With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); lithium iodide; zinc; at 65 ℃; for 8h; Inert atmosphere; Sealed tube; Green chemistry;
DOI:10.1021/acs.orglett.1c04018

Reference yield: 53.0%

: 7486-35-3
tri-n-butyl(vinyl)tin

: 14001-66-2
5-bromo-2-methoxypyrimidine

: 120717-41-1
2-methoxy-5-vinylpyrimidine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In 1,2-dichloro-ethane; for 2h; Heating;

Reference yield:

: 1779-49-3
Methyltriphenylphosphonium bromide

: 90905-32-1
2-methoxy-pyrimidine-5-carbaldehyde

: 120717-41-1
2-methoxy-5-vinylpyrimidine

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.2h;

2-methoxy-pyrimidine-5-carbaldehyde; In tetrahydrofuran; hexane; at 0 - 60 ℃; for 4.5h;