N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

Base Information

Chemical Name:N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine
CAS No.:940941-93-5
Molecular Formula:C₂₃H₃₂BrNSSi
Molecular Weight:462.569
Hs Code.:

Synonyms:N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

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Chemical Property of N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

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Technology Process of N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

There total 1 articles about N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 867218-80-2
chloro(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilane

: 80058-84-0
4-bromo-2,6-diisopropylaniline

: 940941-93-5
N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

Guidance literature:: 4-bromo-2,6-diisopropylaniline; With n-butyllithium; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 1h;

chloro(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilane; In tetrahydrofuran; hexane; at 20 ℃;

Reference yield: 56.0%

: ZrCl₄(THF)2

: 940941-93-5
N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

: dimethylsilanediyl(η5-4,5-dimethylcyclopenta[b]thien-6-yl)(N-(2,6-diisopropyl-4-bromophenylamido))zirconium dichloride

Guidance literature:: N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine; With methyllithium; In diethyl ether; at -30 - 20 ℃; for 4h;

ZrCl₄(THF)2; In diethyl ether; at -80 - 20 ℃; for 24h;

Reference yield: 33.0%

: 940941-93-5
N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine

: 7550-45-0
titanium tetrachloride

: dimethylsilanediyl(η5-4,5-dimethylcyclopenta[b]thien-6-yl)(N-(2,6-diisopropyl-4-bromophenylamido))titanium dichloride

Guidance literature:: N-(4-bromo-2,6-diisopropylphenyl)(4,5-dimethyl-6H-cyclopenta[b]thien-6-yl)dimethylsilanamine; With methyllithium; In diethyl ether; at 20 ℃;

titanium tetrachloride; In diethyl ether; pentane; at 0 - 20 ℃; for 24.5h;