Technology Process of C13H17N4O5P
There total 5 articles about C13H17N4O5P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; ammonium formate;
In
methanol;
for 0.333333h;
Reflux;
DOI:10.1021/jm301577q
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium osmate(VI) dihydrate; sodium periodate / tetrahydrofuran; water / 4 h / Darkness
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C
2.2: 0.25 h / -78 °C
3.1: triphenylphosphine; di-isopropyl azodicarboxylate; sodium azide; sulfuric acid / water; toluene / 2 h / 0 - 20 °C
4.1: copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide; water / 1 h / 80 °C / Microwave irradiation
5.1: ammonium formate; palladium 10% on activated carbon / methanol / 0.33 h / Reflux
With
potassium osmate(VI) dihydrate; sodium periodate; sodium azide; di-isopropyl azodicarboxylate; sulfuric acid; palladium 10% on activated carbon; ammonium formate; copper(II) sulfate; sodium L-ascorbate; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;
3.1: |Mitsunobu Displacement;
DOI:10.1021/jm301577q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C
1.2: 0.25 h / -78 °C
2.1: triphenylphosphine; di-isopropyl azodicarboxylate; sodium azide; sulfuric acid / water; toluene / 2 h / 0 - 20 °C
3.1: copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide; water / 1 h / 80 °C / Microwave irradiation
4.1: ammonium formate; palladium 10% on activated carbon / methanol / 0.33 h / Reflux
With
sodium azide; di-isopropyl azodicarboxylate; sulfuric acid; palladium 10% on activated carbon; ammonium formate; copper(II) sulfate; sodium L-ascorbate; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;
2.1: |Mitsunobu Displacement;
DOI:10.1021/jm301577q