C₄₀H₄₁Cl₂N₅O₉

Base Information

Chemical Name:C₄₀H₄₁Cl₂N₅O₉
CAS No.:1438408-34-4
Molecular Formula:C₄₀H₄₁Cl₂N₅O₉
Molecular Weight:806.7
Hs Code.:

C<sub>40</sub>H<sub>41</sub>Cl<sub>2</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:C₄₀H₄₁Cl₂N₅O₉

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Chemical Property of C₄₀H₄₁Cl₂N₅O₉

Chemical Property:

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Technology Process of C₄₀H₄₁Cl₂N₅O₉

There total 12 articles about C₄₀H₄₁Cl₂N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1438408-33-3
C₂₆H₃₃N₅O₇*ClH

: 41490-13-5
4-(benzyloxy)-3,5-dichlorobenzoicacid

: 1438408-34-4
C₄₀H₄₁Cl₂N₅O₉

Guidance literature:: C₂₆H₃₃N₅O₇*ClH; With N-ethyl-N,N-diisopropylamine; at 0 ℃; Inert atmosphere;

4-(benzyloxy)-3,5-dichlorobenzoicacid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-16-2
C₁₄H₂₅NO₄

: 1438408-34-4
C₄₀H₄₁Cl₂N₅O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 8 h / 20 °C / Inert atmosphere

2.3: 3.33 h / 20 °C / Inert atmosphere

3.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

5.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

9.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

9.2: 3 h / 50 °C / Inert atmosphere

10.1: hydrogenchloride / methanol; water / 10 h / 40 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine / 0 °C / Inert atmosphere

11.2: 0 - 20 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; iodine; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-17-3
C₁₄H₂₄INO₃

: 1438408-34-4
C₄₀H₄₁Cl₂N₅O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

1.3: 3.33 h / 20 °C / Inert atmosphere

2.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

4.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

5.2: 0.5 h / -78 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

7.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

8.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

8.2: 3 h / 50 °C / Inert atmosphere

9.1: hydrogenchloride / methanol; water / 10 h / 40 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / 0 °C / Inert atmosphere

10.2: 0 - 20 °C / Inert atmosphere

With hydrogenchloride; Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 3.1: |Dess-Martin Oxidation / 4.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d