methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate

Base Information

Chemical Name:methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate
CAS No.:1018435-45-4
Molecular Formula:C₂₃H₃₂ClNO₆SSi
Molecular Weight:514.115
Hs Code.:

Synonyms:methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate

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Technology Process of methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate

There total 1 articles about methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1008531-10-9
methyl (2S)-2-hydroxy-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1018435-45-4
methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

Reference yield: 83.0%

: 1018435-45-4
methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate

: 1018435-48-7
(2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionic acid

Guidance literature:: methyl (2S)-2-(tert-butyl-dimethylsilyloxy)-3-{N-[4-(4-chlorophenoxy)phenyl],N-methanesulfonylamino}propionate; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 3h;

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate;