4-(2-(2-Chloroethoxy)ethoxy)benzaldehyde

Base Information

• Chemical Name: 4-(2-(2-Chloroethoxy)ethoxy)benzaldehyde
• CAS No.: 130413-37-5
• Molecular Formula: C₁₁H₁₃ClO₃
• Molecular Weight: 228.675
• European Community (EC) Number: 653-190-8

Synonyms:4-(2-(2-Chloroethoxy)ethoxy)benzaldehyde;130413-37-5;starbld0040693;AKOS024334027;4-(2-(2-CHLOROETHOXY)ETHOXY)-BENZALDEHYDE

Chemical Property of 4-(2-(2-Chloroethoxy)ethoxy)benzaldehyde

Chemical Property:

• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 7
• Exact Mass: 228.0553220
• Heavy Atom Count: 15
• Complexity: 167

Purity/Quality:

4-(2-(2-CHLOROETHOXY)ETHOXY)-BENZALDEHYDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1C=O)OCCOCCCl

Technology Process of 4-(2-(2-Chloroethoxy)ethoxy)benzaldehyde

There total 1 articles about 4-(2-(2-Chloroethoxy)ethoxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) + 3-oxa-1,5-dichloropentane (111-44-4) → 4-(2-(2-chloroethoxy)ethoxy)benzaldehyde (130413-37-5)

Guidance literature:

With potassium carbonate; In acetonitrile; Reflux;

DOI:10.1016/j.biopha.2021.111678

Reference yield: 86.0%

4-(2-(2-chloroethoxy)ethoxy)benzaldehyde (130413-37-5) → 2-(2-(4-formylphenoxy)ethoxy)ethyl nitrate

Guidance literature:

With silver nitrate; In acetonitrile; for 12h; Reflux; Darkness;

DOI:10.1016/j.biopha.2021.111678

Reference yield: 10.0%

pyrrole (109-97-7,30604-81-0) + 4-(2-(2-chloroethoxy)ethoxy)benzaldehyde (130413-37-5) + benzaldehyde (100-52-7) → 5,15,10,20-tetraphenylporphyrin (917-23-7,20998-75-8) + 5-<4-(6-chloro-1,4-dioxahexyl)phenyl>-10,15,20-triphenylporphyrin (99521-97-8) + 5,10-di<4-(6-chloro-1,4-dioxahexyl)phenyl>-15,20-diphenylporphyrin + 5,15-di<4-(6-chloro-1,4-dioxahexyl)phenyl>-10,20-diphenylporphyrin (130413-28-4)

Guidance literature:

With chloroacetic acid; In xylene; for 2h; Heating;

upstream raw materials:

4-hydroxy-benzaldehyde

3-oxa-1,5-dichloropentane

Downstream raw materials:

5,15,10,20-tetraphenylporphyrin

5-<4-(6-chloro-1,4-dioxahexyl)phenyl>-10,15,20-triphenylporphyrin

5,15-di<4-(6-chloro-1,4-dioxahexyl)phenyl>-10,20-diphenylporphyrin

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