N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

Base Information

Chemical Name:N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester
CAS No.:618095-50-4
Molecular Formula:C₂₃H₃₄N₂O₁₀
Molecular Weight:498.53
Hs Code.:

N<sup>α</sup>-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

Synonyms:N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

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Chemical Property of N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

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Technology Process of N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

There total 3 articles about N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1016-58-6
6-nitroveratryl alcohol

: 24277-39-2
N-tert-butoxycarbonyl glutamic acid tert-butyl ester

: 618095-50-4
N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1021/jo035774n

Reference yield:

: 53413-67-5
6-nitroveratrylbromide

: 24277-39-2
N-tert-butoxycarbonyl glutamic acid tert-butyl ester

: 618095-50-4
N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; Inert atmosphere; Darkness;

Reference yield:

: 165811-64-3
4,5-dimethoxy-2-nitrobenzyl 2-aminoacetate hydrochloride

: 618095-50-4
N^α-(tert-butoxycarbonyl)-γ-(6-nitroveratryl)glutamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: (RS)-1-(3,5-dimethoxyphenyl)-2-oxo-2-phenylethyl 4-aminobutanoate hydrochloride / Irradiation; Photolysis

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / Inert atmosphere

With dmap; (RS)-1-(3,5-dimethoxyphenyl)-2-oxo-2-phenylethyl 4-aminobutanoate hydrochloride; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/c1cc15135e