p-Bromzimtsaeure-N,N-dimethylamid

Base Information

Chemical Name:p-Bromzimtsaeure-N,N-dimethylamid
CAS No.:57528-16-2
Molecular Formula:C₁₁H₁₂BrNO
Molecular Weight:254.126
Hs Code.:

Synonyms:p-Bromzimtsaeure-N,N-dimethylamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-Bromzimtsaeure-N,N-dimethylamid

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Technology Process of p-Bromzimtsaeure-N,N-dimethylamid

There total 1 articles about p-Bromzimtsaeure-N,N-dimethylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200-07-3
3-(4-bromophenyl)acrylic acid

: 124-40-3
dimethyl amine

: 57528-16-2
p-Bromzimtsaeure-N,N-dimethylamid

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jacs.0c09654

Reference yield: 95.0%

: 20619-23-2
N,N-diphenylpropionamide

: 57528-16-2
p-Bromzimtsaeure-N,N-dimethylamid

: (2S,3S)-3-(4-bromophenyl)-N₅,N₅,2-trimethyl-N₁,N₁-diphenylpentanediamide

Guidance literature:: With potassium hexamethylsilazane; 8,9,11,12,14,15,17,18,33,34,36,37,39,40,42,43-hexadecahydrotetranaphtho[2,1-e1:1',2'-g1:2'',1''-n:1''',2'''-p][1,4,7,10,13,18,21,24,27,30]decaoxacyclotetratriacontine; In toluene; at -40 ℃; for 15h; Molecular sieve; Inert atmosphere;
DOI:10.1021/jacs.5b01943

Reference yield: 95.0%

: 20619-23-2
N,N-diphenylpropionamide

: 57528-16-2
p-Bromzimtsaeure-N,N-dimethylamid

: 3-(4-bromophenyl)-N⁵,N⁵,2-trimethyl-N¹,N¹-diphenylpentanediamide

Guidance literature:: N,N-diphenylpropionamide; With K/γ-Al₂O₃; In toluene; at -40 ℃; for 0.5h; Glovebox;

p-Bromzimtsaeure-N,N-dimethylamid; In toluene; at -40 ℃; for 36h; diastereoselective reaction; Glovebox;
DOI:10.1002/adsc.201900364