Technology Process of dibenzyl 4-vinylphenyl phosphate
There total 3 articles about dibenzyl 4-vinylphenyl phosphate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-Vinylphenol;
With
dmap; N-ethyl-N,N-diisopropylamine;
In
tetrachloromethane; acetonitrile;
at -10 ℃;
for 0.5h;
Dibenzyl phosphite;
In
tetrachloromethane; acetonitrile;
at -10 - 20 ℃;
DOI:10.1021/ja9060917
- Guidance literature:
-
4-Vinylphenol;
With
dmap; N-ethyl-N,N-diisopropylamine;
In
tetrachloromethane; acetonitrile;
at -10 ℃;
for 0.5h;
Schlenk technique;
dibenzyl hydrogen phosphite;
In
tetrachloromethane; acetonitrile;
at 20 ℃;
Schlenk technique;
DOI:10.1021/jacs.5b02347
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydroxide / tetrahydrofuran / Schlenk technique
1.2: pH 7 / Schlenk technique
2.1: dmap; N-ethyl-N,N-diisopropylamine / acetonitrile; tetrachloromethane / 0.5 h / -10 °C / Schlenk technique
2.2: 20 °C / Schlenk technique
With
dmap; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; tetrachloromethane; acetonitrile;
DOI:10.1021/jacs.5b02347
