N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide

Base Information

Chemical Name:N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide
CAS No.:1431325-89-1
Molecular Formula:C₂₁H₃₄NO₂*I
Molecular Weight:459.411
Hs Code.:

Synonyms:N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide

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Chemical Property of N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide

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Technology Process of N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide

There total 4 articles about N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1431326-49-6
1-(cyclohexyl(methyl)amino)propan-2-yl2-isopropylbenzoate

: 74-88-4
methyl iodide

: 1431325-89-1
N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide

Guidance literature:: In 1,2-dichloro-ethane; at 20 ℃; for 16h; Sealed tube;

Reference yield:

: 103-00-4
1-(cyclohexylamino)-2-propanol

: 1431325-89-1
N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane; water / 16 h / 20 °C / Cooling with ice

2: toluene / 16 h / 0 °C / Reflux

3: 1,2-dichloro-ethane / 16 h / 20 °C / Sealed tube

With sodium tris(acetoxy)borohydride; acetic acid; In water; 1,2-dichloro-ethane; toluene;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1431325-89-1
N-[2-((2-isopropylbenzoyl)oxy)propyl]-N,N-dimethylcyclohexanaminium iodide

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 0.17 h / 0 - 10 °C

1.2: 0.25 h / 0 - 20 °C

2.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane; water / 16 h / 20 °C / Cooling with ice

3.1: toluene / 16 h / 0 °C / Reflux

4.1: 1,2-dichloro-ethane / 16 h / 20 °C / Sealed tube

With sodium tris(acetoxy)borohydride; acetic acid; In ethanol; water; 1,2-dichloro-ethane; toluene;