5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate

Base Information

Chemical Name:5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate
CAS No.:1382490-72-3
Molecular Formula:C₁₈H₁₆O₄
Molecular Weight:296.323
Hs Code.:

Synonyms:5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate

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Chemical Property of 5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate

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Technology Process of 5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate

There total 2 articles about 5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 78326-88-2
5-benzyloxy-1-indanone

: 64-19-7,77671-22-8
acetic acid

: 1382490-72-3
5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate

Guidance literature:: With potassium permanganate; In benzene; Reflux; Dean-Stark;
DOI:10.1021/jo300850a

Reference yield:

: 3470-49-3
5-hydroxy-2,3-dihydro-1H-indene-1-one

: 100-39-0
benzyl bromide

: 1382490-72-3
5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 20 °C

2: potassium permanganate / benzene / Reflux; Dean-Stark

With potassium permanganate; potassium carbonate; In acetonitrile; benzene;
DOI:10.1021/jo300850a

Reference yield:

: 1382490-72-3
5-(benzyloxy)-2,3-dihydro-1-oxo-1H-inden-2-yl acetate

: 38005-82-2
2,3-dihydro-1H-indene-1,5-diol

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C

2: [D₃]acetonitrile; water-d2 / Photolysis

3: sodium tetrahydroborate / d⁽⁴⁾-methanol / 0 °C / Inert atmosphere

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; In d⁽⁴⁾-methanol; [D₃]acetonitrile; water-d2; ethyl acetate;
DOI:10.1021/jo300850a