O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate

Base Information

Chemical Name:O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate
CAS No.:119447-81-3
Molecular Formula:C₃₅H₃₄Cl₃NO₅S
Molecular Weight:687.084
Hs Code.:

Synonyms:O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate

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Technology Process of O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate

There total 3 articles about O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 117901-42-5
3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 119447-81-3
O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate

Guidance literature:: With sodium hydride; In dichloromethane; Ambient temperature;
DOI:10.1055/s-1988-27673

Reference yield:

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 119447-81-3
O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) Na₂CO₃ / 1.) CCl₄, room temp., 2.) THF, H₂O, room temp., 0.5 h; room temp. to 50 deg C, 1 h

2: 70 percent / NaH / CH₂Cl₂ / Ambient temperature

With sodium hydride; sodium carbonate; In dichloromethane;
DOI:10.1055/s-1988-27673

Reference yield:

: 931-59-9
benzenesulfenyl chloride

: 119447-81-3
O-(3,4,6-Tri-O-benzyl-2-deoxy-2-phenylthio-α-D-glucopyranosyl)trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) Na₂CO₃ / 1.) CCl₄, room temp., 2.) THF, H₂O, room temp., 0.5 h; room temp. to 50 deg C, 1 h

2: 70 percent / NaH / CH₂Cl₂ / Ambient temperature

With sodium hydride; sodium carbonate; In dichloromethane;
DOI:10.1055/s-1988-27673