(E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane

Base Information

Chemical Name:(E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane
CAS No.:1239335-36-4
Molecular Formula:C₃₃H₃₄O₂S
Molecular Weight:494.698
Hs Code.:

Synonyms:(E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane

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Chemical Property of (E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane

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Technology Process of (E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane

There total 1 articles about (E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1239335-35-3
(E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl trifluoromethane sulfonate

: 75-66-1
2-methylpropan-2-thiol

: 1239335-36-4
(E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane

Guidance literature:: (E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl trifluoromethane sulfonate; With palladium diacetate; (R)-tol-BINAP; In toluene; at 20 ℃; for 0.25h;

2-methylpropan-2-thiol; With sodium hexamethyldisilazane; In toluene; at 20 - 100 ℃; Inert atmosphere;
DOI:10.3390/molecules15085595

Reference yield: 86.0%

: 1239335-36-4
(E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane

: 1239335-37-5
(1S,2S)-1-(3',4'-bis(benzyloxy)phenyl)-3-(2-tert-butylthiophenyl)propane-1,2-diol

Guidance literature:: (E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane; With AD-mix-α; In dichloromethane; water; tert-butyl alcohol; at 0 ℃;

With methanesulfonamide; In dichloromethane; water; tert-butyl alcohol; at 0 ℃; for 24h; optical yield given as %ee;
DOI:10.3390/molecules15085595

Reference yield: 83.0%

: 1239335-36-4
(E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane

: 1239335-40-0
(1R,2R)-1-(3',4'-bis(benzyloxy)phenyl)-3-(2-(tert-butylthio)phenyl)propane-1,2-diol

Guidance literature:: (E)-2-(3-(3',4'-bis(benzyloxy)phenyl)allyl)phenyl-tert-butylsulfane; In dichloromethane; water; tert-butyl alcohol; at 0 ℃;

With methanesulfonamide; In dichloromethane; water; tert-butyl alcohol; at 0 ℃; for 24h;
DOI:10.3390/molecules15085595