(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt

Base Information

Chemical Name:(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt
CAS No.:1173158-19-4
Molecular Formula:C₂HF₃O₂*C₂₀H₃₉N₃O₄
Molecular Weight:499.571
Hs Code.:

Synonyms:(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt

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Chemical Property of (2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt

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Technology Process of (2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt

There total 5 articles about (2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1173158-21-8
C₂₄H₄₃N₃O₆

: 76-05-1
trifluoroacetic acid

: 1173158-19-4
(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt

Guidance literature:: C₂₄H₄₃N₃O₆; With diethylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In water; acetonitrile; at 22 ℃; for 1h;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 1173157-89-5
6-(prop-2-enyl-butyloxycarbonyl-amino)hexylmethyl sulfonate

: 1173158-19-4
(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / diethyl ether / 0 - 22 °C

2.1: hydrogenchloride / diethyl ether / 5 h / 22 °C

3.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.25 h / 22 °C

3.2: 1 h

4.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylamine; N-ethyl-N,N-diisopropylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In diethyl ether; dichloromethane; water; acetonitrile;

Reference yield:

: 146292-92-4
N-(6-hydroxy-hexyl)prop-2-enyloxycarboxamide

: 1173158-19-4
(2R)-N-(6-aminohexyloxy)-2-[(tert-butoxy)carbonylamino]-3-cyclohexylpropanamide trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 0 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / diethyl ether / 0 - 22 °C

3.1: hydrogenchloride / diethyl ether / 5 h / 22 °C

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.25 h / 22 °C

4.2: 1 h

5.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 1 h / 22 °C

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; In diethyl ether; dichloromethane; water; acetonitrile;