1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

Base Information

• Chemical Name: 1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate
• CAS No.: 68967-65-7
• Molecular Formula: C₁₆H₂₄INO₃
• Molecular Weight: 405.276

Synonyms:1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

Chemical Property of 1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

Chemical Property:

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Technology Process of 1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

There total 2 articles about 1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2-aminomethyl-4-tert-butyl-6-iodophenol (58456-91-0) + 1,1-dimethylethyl 2,4,5-trichlorophenyl carbonate (16965-08-5) → 1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate (68967-65-7)

Guidance literature:

With triethylamine; In tetrahydrofuran; water; at 60 - 65 ℃; for 24h;

DOI:10.1021/jm00348a024

Reference yield:

→ 1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate (68967-65-7)

Guidance literature:

2-Aminomethyl-4-(1,1-dimethylaethyl)-6-iod-phenol, (1,1-Dimethylaethyl)oxycarbonylazid, MgO;

Reference yield: 63.0%

1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate (68967-65-7) + dimethylamino sulfonyl chloride (13360-57-1) → 2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate (68967-66-8)

Guidance literature:

With triethylamine; In dichloromethane; at 20 - 25 ℃; for 72h;

DOI:10.1021/jm00348a024

upstream raw materials:

2-aminomethyl-4-tert-butyl-6-iodophenol

1,1-dimethylethyl 2,4,5-trichlorophenyl carbonate

Downstream raw materials:

(5-tert-Butyl-2-carbamoylmethoxy-3-iodo-benzyl)-carbamic acid tert-butyl ester

(5-tert-Butyl-2-ethylsulfamoyloxy-3-iodo-benzyl)-carbamic acid tert-butyl ester

2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

2-<2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenoxy>acetamide hydrochloride

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