2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

Base Information

Chemical Name:2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide
CAS No.:1382669-33-1
Molecular Formula:C₁₉H₂₇NO₃
Molecular Weight:317.428
Hs Code.:

Synonyms:2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

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Chemical Property of 2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

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Technology Process of 2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

There total 3 articles about 2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1382669-30-8
2-((1R,5S)-5-(2-hydroxyethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

: 824-94-2
p-methoxybenzyl chloride

: 1382669-33-1
2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

Guidance literature:: 2-((1R,5S)-5-(2-hydroxyethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 24h;
DOI:10.1007/s00726-011-0925-z

Reference yield:

: 120052-54-2
(1S,3S)-1-hydroxy-3-(methyl-carboxymethyl)-4-cyclopentene

: 1382669-33-1
2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Heating

2.1: lithium borohydride / tetrahydrofuran; diethyl ether / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

3.2: 24 h / 20 °C

With lithium borohydride; sodium hydride; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; N,N-dimethyl-formamide; mineral oil;
DOI:10.1007/s00726-011-0925-z

Reference yield:

: 128740-98-7
methyl 2-((1S,2R)-2-(2-(dimethylamino)-2-oxoethyl)cyclopent-3-en-1-yl)acetate

: 1382669-33-1
2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium borohydride / tetrahydrofuran; diethyl ether / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

2.2: 24 h / 20 °C

With lithium borohydride; sodium hydride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; mineral oil;
DOI:10.1007/s00726-011-0925-z