((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane

Base Information

Chemical Name:((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane
CAS No.:1382669-45-5
Molecular Formula:C₂₉H₅₄O₄Si₂
Molecular Weight:522.916
Hs Code.:

Synonyms:((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane

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Chemical Property of ((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane

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Technology Process of ((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane

There total 7 articles about ((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 994-30-9
triethylsilyl chloride

: 1382669-42-2
(1S,2R,3S)-2-(2-hydroxyethyl)-3-(2-((4-methoxybenzyl)oxy)ethyl)cyclopentanol

: 1382669-45-5
((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1007/s00726-011-0925-z

Reference yield:

: 1382669-33-1
2-((1R,5S)-5-(2-((4-methoxybenzyl)oxy)ethyl)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

: 1382669-45-5
((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane

Guidance literature:: Multi-step reaction with 4 steps

1: iodine / tetrahydrofuran; water / 3 h / 20 °C

2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / Heating

3: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C

4: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); iodine; tri-n-butyl-tin hydride; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide; benzene;
DOI:10.1007/s00726-011-0925-z

Reference yield:

: 1382669-36-4
(3aR,4R,6R,6aR)-6-iodo-4-(2-((4-methoxybenzyl)oxy)ethyl)hexahydro-2H-cyclopenta[b]furan-2-one

: 1382669-45-5
((1S,2R,3S)-3-(2-((4-methoxybenzyl)oxy)ethyl)-2-(2-((triethylsilyl)oxy)ethyl)-1-((triethylsilyl)oxy))cyclopentane

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / Heating

2: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In diethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.1007/s00726-011-0925-z